Synthesis of Nanocrystals of Long Persisting Phosphor by Modified Combustion Technique

Abstract

Synthesis and characterization of Nanocrystalline long persistent SrAl2O4:Eu2+, Dy3+ phosphor via a modified combustion process has been presented in the paper. In this synthesis process, a mixture of respective metal nitrates, flux and combustible agent (urea/camphor) were thermally treated with slight modification at 400-600oC for about 5 minutes. It resulted in low-density voluminous mass in contrast to a solid lump by conventional solid-state method. The present work reports the changes made in the combustion process to achieve the homogenous incorporation of dopants and large-scale production of the nanophosphor in a short interval of time. The samples have been characterized for nanophase, structural and luminescent properties. PACS Code: 33.50.-j, 33.50.Dq, 78.55.-m, 68.37.Hk